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Home > Products >  China Largest Factory Manufacturer sales Dibenzoyl-L-tartaric acid monohydrate CAS 62708-56-9

China Largest Factory Manufacturer sales Dibenzoyl-L-tartaric acid monohydrate CAS 62708-56-9 CAS NO.62708-56-9

  • FOB Price: USD: 1.00-2.00 /Kilogram Get Latest Price
  • Min.Order: 500 Kilogram
  • Payment Terms: L/C,D/A,D/P,T/T,MoneyGram,Other
  • Available Specifications:

    AAAAA(50-100)KilogramAAAAA(100-500)Kilogram

  • Product Details

Keywords

  • Dibenzoyl-L-tartaric acid monohydrate
  • Dibenzoyl-L-tartaric acid monohydrate
  • 62708-56-9

Quick Details

  • ProName: China Largest Factory Manufacturer sal...
  • CasNo: 62708-56-9
  • Molecular Formula: 62708-56-9
  • Appearance: white powder
  • Application: Pharm chemicals industry
  • DeliveryTime: 3-5 days
  • PackAge: 25KG/Drum
  • Port: Shanghai Guangzhou Qingdao Shenzhen
  • ProductionCapacity: 20 Metric Ton/Month
  • Purity: 99%
  • Storage: 2-8°C
  • Transportation: By air /Sea/ coruier
  • LimitNum: 500 Kilogram
  • Heavy metal: 10PPM
  • Color: white
  • Melting point: ≥350°C
  • Boiling point: 363.24°C (rough estimate)
  • density: 1.667
  • solubility: 1 M NaOH: 10 mg/mL, dark green
  • Water Solubility: <0.1 g/100 mL at 21 oC
  • Stability: Stable. Combustible. Incompatible with...

Superiority

                                PRODUCT DETAILS       

(-)-Dibenzoyl-L-tartaric acid monohydrate Basic information
Product Name: (-)-Dibenzoyl-L-tartaric acid monohydrate
Synonyms: L-(-)DIBENZOYL-L-TARTARIC ACID 1-HYDRATE;(2S,3S)-2,3-bis(benzoyloxy)succinic acid hydrate;O,O'-Dibenzoyl-d-Tartaric acid Anhydrous;(-)-O,O''-DIBENZOYL-L-WEINSUREMONOHYDRAT;DIBENZOYL-L-TARARIC ACID MOTOHYDRATE;(-)-Dibenzoyl-L-tartaric acid Monohydrate, 98% 100GR;(2R,3R)-(-)-DI-O-BENZOYL-TARTARIC ACID M;Dibenzoyl-L-tartaric acid Monohydrat
CAS: 62708-56-9
MF: C18H16O9
MW: 376.31
EINECS: 613-072-9
Product Categories: chiral;Pharmaceutical Intermediates;FINE Chemical & INTERMEDIATES;Carboxylic Acids (Chiral);Chiral Building Blocks;Widely used in chiral especially racemic amine compounds;for Resolution of Bases;Optical Resolution;Synthetic Organic Chemistry;CHIRAL CHEMICALS;Hydroxy Acids & Deriv.;Chiral Compound;Carboxylic AcidsAsymmetric Synthesis;Chiral Building Blocks;Chiral Resolution Reagents;Chiral Resolving Reagents;Organic Building Blocks
Mol File: 62708-56-9.mol
(-)-Dibenzoyl-L-tartaric acid monohydrate Structure
 
(-)-Dibenzoyl-L-tartaric acid monohydrate Chemical Properties
Melting point  88-89 °C(lit.)
alpha  -115 º (c=5, ethanol)
refractive index  -108.5 ° (C=1, EtOH)
storage temp.  Store below +30°C.
form  Powder
color  White
optical activity [α]20/D 110±3°, c = 5% in ethanol
Water Solubility  SOLUBLE
BRN  4065263
InChIKey DXDIHODZARUBLA-DTPOWOMPSA-N
CAS DataBase Reference 62708-56-9(CAS DataBase Reference)
 
Safety Information
Hazard Codes  Xi
Risk Statements  36
Safety Statements  26-36-37/39
WGK Germany  3
RTECS  WW8070000
3
TSCA  Yes
HS Code  29181990
MSDS Information
Provider Language
SigmaAldrich English
ACROS English
ALFA English
 
(-)-Dibenzoyl-L-tartaric acid monohydrate Usage And Synthesis
Chemical Properties white to light yellow crystal powde
Uses (-)-Dibenzoyl-L-tartaric acid is used as an intermediate in pharmaceutical and agro chemical industries. It is used as chiral auxiliary in organic synthesis and as a resolution agent in the synthesis of rameleton.
General Description (-)-O,O′-Dibenzoyl-L-tartaric acid monohydrate may be used as a chiral resolving agent for the resolution of racemic bioactive compounds such as (±)-3-(3-hydroxyphenyl)-N-(1-propyl)-piperidine and (±)-2-(5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthyl)-imidazoline to isolate the corresponding (-)-enantiomeric forms.
Purification Methods Crystallise the acid from water (18g from 400 mL boiling H2O) and stir vigorously while cooling in order to obtain crystals; otherwise an oil will separate which solidifies on cooling. Dry it in a vacuum desiccator over KOH/H2SO4 (yield 16.4g) as monohydrate, m 88-89o. It crystallises from xylene as the anhydrous acid, m 173o (150-153o). It does not crystallise from *C6H6, toluene, *C6H6/pet ether (oil), or CHCl3/pet ether. [Butler & Cretcher J Am Chem Soc 55 2605 1933, Acs et al. Tetrahedron 41 2465 1985, R(+) Beilstein 9 IV 557, S(-) Beilstein 9 III 870.]
 
(-)-Dibenzoyl-L-tartaric acid monohydrate Preparation Products And Raw materials


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Leader Biochemical Group is a large leader incorporated industry manufacturers and suppliers of advanced refined raw materials From the year of 1996 when our factory was put into production to year of 2020, our group has successively invested in more than 52 factories with shares and subordinates.We focus on manufacture Pharm & chemicals, functional active ingredients, nutritional Ingredients, health care products, cosmetics, pharmaceutical and refined feed, oil, natural plant ingredients industries to provide top quality of GMP standards products.All the invested factories' product lines cover API and intermediates, vitamins, amino acids, plant extracts, daily chemical products, cosmetics raw materials, nutrition and health care products, food additives, feed additives, essential oil products, fine chemical products and agricultural chemical raw materials And flavors and fragrances. Especially in the field of vitamins, amino acids, pharmaceutical raw materials and cosmetic raw materials, we have more than 20 years of production and sales experience. All products meet the requirements of high international export standards and have been recognized by customers all over the world. Our manufacture basement & R&D center located in National Aerospace Economic & Technical Development Zone Xi`an Shaanxi China. Now not only relying on self-cultivation and development as well as maintains good cooperative relations with many famous research institutes and universities in China. Now, we have closely cooperation with Shanghai Institute of Organic Chemistry of Chinese Academy of Science, Beijing Institute of Material Medical of Chinese Academy of Medical Science, China Pharmaceutical University, Zhejiang University. Closely cooperation with them not only integrating Science and technology resources, but also increasing the R&D speed and improving our R&D power. Offering Powerful Tech supporting Platform for group development. Keep serve the manufacture and the market as the R&D central task, focus on the technical research.  Now there are 3 technology R & D platforms including biological extract, microorganism fermentation and chemical synthesis, and can independently research and develop kinds of difficult APIs and pharmaceutical intermediates. With the strong support of China State Institute of Pharmaceutical Industry (hereinafter short for CSIPI), earlier known as Shanghai Institute of Pharmaceutical Industry (SIPI), we have unique advantages in the R & D and industrialization of high-grade, precision and advanced products.  Now our Group technical force is abundant, existing staff more that 1000 people, senior professional and technical staff accounted for more than 50% of the total number of employees, including 15 PhD research and development personnel, 5 master′ S degree in technical and management personnel 9 people. We have advanced equipment like fermentation equipment and technology also extraction, isolation, purification, synthesis with rich production experience and strict quality control system, According to the GMP required, quickly transforming the R&D results to industrial production in time, it is our advantages and our products are exported to North and South America, Europe, Middle East, Africa, and other five continents and scale the forefront in the nation, won good international reputation.  We believe only good quality can bring good cooperation, quality is our key spirit during our production, we are warmly welcome clients and partner from all over the world contact us for everlasting cooperation, Leader will be your strong, sincere and reliable partner in China.

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                                                       Product information

(-)-Dibenzoyl-L-tartaric acid monohydrate Basic information
Product Name: (-)-Dibenzoyl-L-tartaric acid monohydrate
Synonyms: L-(-)DIBENZOYL-L-TARTARIC ACID 1-HYDRATE;(2S,3S)-2,3-bis(benzoyloxy)succinic acid hydrate;O,O'-Dibenzoyl-d-Tartaric acid Anhydrous;(-)-O,O''-DIBENZOYL-L-WEINSUREMONOHYDRAT;DIBENZOYL-L-TARARIC ACID MOTOHYDRATE;(-)-Dibenzoyl-L-tartaric acid Monohydrate, 98% 100GR;(2R,3R)-(-)-DI-O-BENZOYL-TARTARIC ACID M;Dibenzoyl-L-tartaric acid Monohydrat
CAS: 62708-56-9
MF: C18H16O9
MW: 376.31
EINECS: 613-072-9
Product Categories: chiral;Pharmaceutical Intermediates;FINE Chemical & INTERMEDIATES;Carboxylic Acids (Chiral);Chiral Building Blocks;Widely used in chiral especially racemic amine compounds;for Resolution of Bases;Optical Resolution;Synthetic Organic Chemistry;CHIRAL CHEMICALS;Hydroxy Acids & Deriv.;Chiral Compound;Carboxylic AcidsAsymmetric Synthesis;Chiral Building Blocks;Chiral Resolution Reagents;Chiral Resolving Reagents;Organic Building Blocks
Mol File: 62708-56-9.mol
(-)-Dibenzoyl-L-tartaric acid monohydrate Structure
 
(-)-Dibenzoyl-L-tartaric acid monohydrate Chemical Properties
Melting point  88-89 °C(lit.)
alpha  -115 º (c=5, ethanol)
refractive index  -108.5 ° (C=1, EtOH)
storage temp.  Store below +30°C.
form  Powder
color  White
optical activity [α]20/D 110±3°, c = 5% in ethanol
Water Solubility  SOLUBLE
BRN  4065263
InChIKey DXDIHODZARUBLA-DTPOWOMPSA-N
CAS DataBase Reference 62708-56-9(CAS DataBase Reference)
 
Safety Information
Hazard Codes  Xi
Risk Statements  36
Safety Statements  26-36-37/39
WGK Germany  3
RTECS  WW8070000
3
TSCA  Yes
HS Code  29181990
MSDS Information
Provider Language
SigmaAldrich English
ACROS English
ALFA English
 
(-)-Dibenzoyl-L-tartaric acid monohydrate Usage And Synthesis
Chemical Properties white to light yellow crystal powde
Uses (-)-Dibenzoyl-L-tartaric acid is used as an intermediate in pharmaceutical and agro chemical industries. It is used as chiral auxiliary in organic synthesis and as a resolution agent in the synthesis of rameleton.
General Description (-)-O,O′-Dibenzoyl-L-tartaric acid monohydrate may be used as a chiral resolving agent for the resolution of racemic bioactive compounds such as (±)-3-(3-hydroxyphenyl)-N-(1-propyl)-piperidine and (±)-2-(5,6-dimethoxy-1,2,3,4-tetrahydro-1-naphthyl)-imidazoline to isolate the corresponding (-)-enantiomeric forms.
Purification Methods Crystallise the acid from water (18g from 400 mL boiling H2O) and stir vigorously while cooling in order to obtain crystals; otherwise an oil will separate which solidifies on cooling. Dry it in a vacuum desiccator over KOH/H2SO4 (yield 16.4g) as monohydrate, m 88-89o. It crystallises from xylene as the anhydrous acid, m 173o (150-153o). It does not crystallise from *C6H6, toluene, *C6H6/pet ether (oil), or CHCl3/pet ether. [Butler & Cretcher J Am Chem Soc 55 2605 1933, Acs et al. Tetrahedron 41 2465 1985, R(+) Beilstein 9 IV 557, S(-) Beilstein 9 III 870.]
 
(-)-Dibenzoyl-L-tartaric acid monohydrate Preparation Products And Raw materials

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